Vacuum heat treating at home

Storm_Eagle

Registered
Registered
Joined
Mar 31, 2023
Messages
21
Hi. I want to make a custom ball bearing and want to make the race my self. So i was thinking about making it from tool steel and harden it in a vacuum tube to avoid oxidation. So i think i want to rig up a quartz glass tube that i cap in both ends and wrap a induction coil around the tube and suspend the part to be heated in the tube and purge it with argon and then pull a vacuum in it. And have the bottom of the tube filled with oil and drop the part into that after heating it with the induction heater.

And i was wondering if i can machine the part to the final dimension in the annealed state and not having to grind it after the heat treatment? Because in the vacuum it will not oxidize and it should not warp if it is a round uniform shape right?
 
An interesting idea. My guess. I wouldn't expect a precision surface like a bearing race to hold its shape after quenching, partcularly in this case because you have no control over the uniformity of the quench. Some portions will cool quicker than others and shrink in the process giving rise to stress as the remainder of the part cools and shrinks.

How do you intend to suspend the part while heating?
 
Quenching would produce a lot of oil vapor and gaseous decomposition products. If the pump was able to keep up with them, there shouldn't be a problem.
 
Quenching would produce a lot of oil vapor and gaseous decomposition products. If the pump was able to keep up with them, there shouldn't be a problem.
Why would i keep the vacuum pump running? When the part has quenched there would be no point in having the vacuum any more. The part has then cooled down and is in the oksygen free environment of the oil bath. I was thinking i would just shut off the vacuum inlet valve when it is pumped down to vacuum and turn off the pump before starting the induction heating.

If there is a chanse there will be a overpressure from the oil gasses i guess i could add a check valve as well that can vent any overpressure.
 
Last edited:
If the part was very small (under half inch) perhaps... , but I forsee a problem heating the part shaped like a bearing race evenly with induction coils. It would have to be suspended horizontally. (same plane of rotation as the coil). This complicated the release and quench mechanism somewhat.

Also, why use vacuum if you're going to use oil for quenching? Why not just fill it with argon at slight overpressure? This way your tube wouldn't have to be vacuum tight making it a lot simpler. However I doubt a part could be quenched in oil evenly enough to be used as a bearing race as is.

If you have no ability to precision grind it is much easier to plan for hard turning (with cheap Chinese CBN for example) after heat treat, rather then relying on no warpage). Still, a bearing race is a difficult project. I would suggest something else for a start.

Vacuum heat treatment is used not only because vacuum is good at preventing oxidation, but also because it enables use of gas quenching which quenches the parts from all sides at the same time with no need for any movement. If I wanted to experiment with small scale vacuum heat treatment I would do it with gas quenching rather than oil for sure. One could use argon, nitrogen or maybe even carbon dioxide (due to low cost) under pressure for the quench. Instead of using heat exchangers and sending the gas in a loop like they do in big furnaces. One could just expand the pressurised gas into an intermediate chamber to pre cool it and send it through the furnace still at significant overpressure (few bar) to assist venting. And vent the furnace to atmosphere. Now that I think about it, maybe the whole thing could be done without vacuum in the first place if the furnace is small...

Make your tube in a way that you have your inert gas port on bottom end, have an overpressure gate that will blow open and stay open at a certain overpressure (let's say 1.3 bar) on top. Have a large diameter (1in) copper expansion chamber next to your inert gas inlet on the bottom. And have a tiny hole in the chamber on top to allow argon to flow slowly, but have it small enough it doesn't prevent buildup of pressure when lots of gas is introduced.

Put, let's say constant flow of argon at 5l/min through the furnace tube. Do your heating cycle. When ready to quench send your pressurised quenching gas from a high pressure bottle, through a high pressure regulator (there are nitrogen regulators available that can be set up to 50 bar on the low side) through a nozzle into that expansion chamber, the moment the pressure in the tube reaches 1.3 bar the valve on the other end blows open. Your cold gas flow does the quench. Job done.

If I was serious about it I would look for literature on gas quenching first. I would be very surprised if there isn't a lot of research on this.
 
I was thinking just some stainless steel wire with some kind of release mechanism that can be triggered from the outside of the vacuum chamber.
You could attach a steel washer to the end of the wire and secure it from the outside of the tube with a magnet, remove the magnet and the piece will drop.
 
Back
Top